Effect of water of crystallization on synthesis of nanocrystalline ceria by non-hydrolytic method

نویسندگان

  • M. Kamruddin
  • P. K. Ajikumar
  • R. Nithya
  • G. Mangamma
  • A. K. Tyagi
  • Baldev Raj
چکیده

Nanocrystalline ceria has been synthesized by a non-hydrolytic method using organic solvent and precipitant. The effect of the source compound on final nanocrystalline powder was investigated. The cerium nitrate hexahydrate subjected to different vacuum/thermal treatments to get cerium source compound having different extent of water of crystallization. The nanoceria, synthesized from these compounds was characterized by TGA-MS, XRD, HR-TEM and AFM. D 2005 Elsevier B.V. All rights reserved.

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تاریخ انتشار 2005